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How does amperometry work in electrochemical analysis?

Amperometry is an electrochemical technique where the current is measured at a fixed potential over time to study the concentration of an analyte. It is widely used in sensors, biosensors, and analytical chemistry. Here’s a clear explanation:


1. Setup

  • Working electrode: Where the oxidation or reduction of the analyte occurs.
  • Reference electrode: Maintains a stable potential.
  • Counter electrode: Completes the circuit.
  • Electrolyte solution: Contains the analyte to be measured.

2. How it works

  1. A fixed potential is applied to the working electrode, chosen so that only the target analyte undergoes oxidation or reduction.
  2. The analyte reacts at the electrode surface, producing electrons, which generate a current.
  3. This current is proportional to the concentration of the analyte in the solution.
  4. By recording the current over time, changes in analyte concentration can be monitored.

3. Key Points

  • The current depends on diffusion of the analyte to the electrode surface.
  • Amperometry is very sensitive and can detect low concentrations.
  • It is widely used in glucose sensors, environmental monitoring, and drug analysis.

4. Example

  • In a glucose biosensor, glucose is oxidized at the electrode surface, generating a current. The magnitude of this current indicates the glucose concentration in blood.

In simple words: Amperometry measures how fast electrons flow when a specific reaction happens at a fixed voltage, which tells us the amount of a chemical present.

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