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What are the basic principles of volumetric analysis?

The basic principles of volumetric analysis are simple ideas that guide how titrations are done to find the concentration of a substance.

  1. Chemical reaction:
    • The titration is based on a known chemical reaction between the analyte (unknown solution) and the titrant (solution of known concentration).
    • The reaction should be fast, complete, and definite.
  2. Stoichiometry:
    • The amount of reactant used is calculated using the molar ratio from the balanced chemical equation.
    • This allows determination of the concentration of the unknown solution.
  3. Accurate measurement of volume:
    • Precise volumes of the titrant and analyte are measured using burettes, pipettes, and volumetric flasks.
  4. Detection of end point:
    • An indicator or instrumental method is used to detect when the reaction is complete (end point).
  5. Standard solution:
    • The titrant must be a solution of known concentration, called a standard solution.
    • It can be primary standard (highly pure and stable) or secondary standard (standardized against a primary standard).

In short:
Volumetric analysis works on a known chemical reaction, accurate measurement of volume, stoichiometry, and detecting the end point to find the concentration of an unknown solution.

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